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    Routine Determination of Mirex and Photomirex in Fish Tissue in the Presence of Polychlorinated Biphenyls

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    Author
    Insalaco, Samuel E.
    Keyword
    WRT
    Mirex
    Photomirex
    Fish Tissue
    Analysis
    Date Published
    1979-12-01
    
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    URI
    http://hdl.handle.net/20.500.12648/4569
    Abstract
    A procedure for the routine determination of Mirex and Photomirex in fish tissue is described which provides rapid analysis and confirmation using conventional gas chromatographic/electron capture detection (GC/ECD) methods. Coeluting intereferences (i.e. PCB's) are nitrated al lowing for simple separation from Mirex analogs by column chromatography. In Chinook SaImon tissue (Oncorhynchus tshawytscha), PCB removaI averaged 78% and Mirex and Photomirex recoveries were 91% and 86%, respectively. The method has been used successfully for trace analysis of Mirex levels as low as 100 pg.
    Description
    Repository staff redacted information not essential to the integrity of this thesis to protect privacy.
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